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Pagc 2 I of a I <br />Pcmiit No. �\�A-003197-G <br />Moditic:uinn Da[c: �lav I. 20(17 <br />S:mi lint� and itenortin� Requirementc <br />All rcporis for cfllucnt charac[criration or compliancc monitoring shall bc <br />submiucJ in acmrdancc n�ith thc most rcccN vcrsion of Dcpanment of Ecolog�� <br />Publication k 1'1'Q-R-95-R0, l.ahor•afay Ciuidnr+cc nnd !4'l�nlc F.Jfluenr Tn.ricin� <br />7i�.rr R���dcir ('rircrirr, in rcgards lo forntat and contcnt. Rcporls shall coniain <br />hcnch shceis and refcrence to�icant results for test methods. If thc lab proeiJcs <br />the �o�icit�• test Jata on iloppy disk for electronic entry into the Uepanment's <br />dalabase, then thc Permillcc shall srnd the disk to ihe Department �lone with <br />the test reporl, brnch sheets, and relrrence tosicant rcsults. <br />2. l�csline shall bc conductcd on grab samplcs. Grah samples must be shippeJ <br />on icc to �hc lal, immediatcl�' upon colleclion. II a erab sample is received at <br />ihe testine lab �� ithin one hour �fler collection, it must have � temperalure <br />belo�� 20� C at reccipt. If:� grab sample is recci��ed at �he te;tin� lab ��ithin <br />4 hours aflcr collcc�iun, it must hc hcloa 12° C al rcccipt. All othcr samplcs <br />nwst be belou 8° C at re�ript. 'I he lab shall bcein ihe to�icii�• �esting as suon <br />as possible but no I�ter than +6 hours �fler sampling �eas enJed. Thc lab shall <br />storc all samples ai 4° C in the dark from reccipt umil complction ofthc �esi. <br />3. All samplcs and tcst solutions for to�iciq Ic�ting shall havc watcr quality <br />measurements as specificd in Depannunt of Fcology Publication <br />�'\1'Q-R-95-80. /.nhnrarun• Guiduncr unrt 117toh� F.Jllurn! lu.rrcr(v %i�.ct /lr��r���r <br />Crircriu, or most rcccnt �crsiun thercof: <br />�3. rUl to�icitc tests shall mcct qu;�lih• assurancc critcria and �cst condi�ions in thc <br />most rcccnt vcrsians of thc LPA manual lisred in �ubscction A and thc <br />Dcparlmcnl of Eculog)' Publicalion �\VQ-R-9J-S0. Lohnrnton' (it�iduricr uitd <br />If'hulr F�h�rnr To.ricity 7i�.cr Reri��iv Crilerin. 1?.PA'S current pro�edurc manual <br />is L• PA-821-R-02-012. ,11elhud.�, fiir Alru.ctiring rlic :l curr r,�.�;�•;n� ��j r11t�,��„�., <br />cu�d Ki�a�irin�� 11'iUencln Frr.chu uli�r a�id �tlurir�i� lJr,ccnti.ants _ ii�, lid.. Octnbcr <br />2002. Iftest rcsults ar� Jcicnnined to he invalid or anomalous bv �hc <br />I)epannum. Icsting shall he repeated �cith Ireshly colleclyd elllucnt. <br />>. Control ��alcr anJ dilulion watcr shall bc labor;nory �va�cr mccting �hc <br />reyuiremen�s ol�thc I:Pr1 manual listed in suhscclion A or �iristinc n;Uur:�l �+:iter <br />of sutlicicnt yu�+liry� for guod cuntrol perfonnancc. <br />ti. I'hc ��holc cillucnt tosici�y Icsts shnll hc run on an unntodilicd samplc uf linal <br />clllucnt. <br />Thc Pcrmincc mn�� choosc �n conduct n tidl dilution scrics icst during <br />compliancc monitoring in orJcr �o dctcnninc dasc responsc. In this casc. ihc <br />scrics must ha��c a minimum of fi�-c (5) efllucnt conccnlrations and a conirol. <br />l�hc scrics of crnucnirations must includc thc ACGC. <br />