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SECTION 5 - SAMPLING AND ANALYTICAL REQUIREMENTS <br /> 5.1 Sampling Requirements for Users. <br /> A. A minimum of four (4) grab samples must be used for pH, cyanide, total phenols, <br /> oil and grease, sulfide, and volatile organics. The Director will determine on a <br /> case-by-case whether the user will be able to composite the individual grab <br /> samples. For all other pollutants, 24-hour composite samples must be obtained <br /> through flow-proportional composite sampling techniques where feasible. The <br /> City may waive flow-proportional composite sampling for any user that <br /> demonstrates that flow-proportional is not feasible. In such cases, samples may be <br /> obtained through time-proportional composite sampling techniques or through a <br /> minimum of four (4) grab samples where the user demonstrates that this will <br /> provide a representative sample of the effluent being discharged. <br /> B. Samples should be taken immediately downstream from pretreatment facilities if <br /> such exist or immediately downstream from the regulated or manufacturing <br /> process if no pretreatment exists or as determined by the City and/or contained in <br /> the user's wastewater discharge permit. For categorical users, if other wastewaters <br /> are mixed with the regulated wastewater prior to pretreatment the user shall <br /> measure the flows and concentrations necessary to allow use of the combined <br /> wastestream formula of 40 CFR 403.6(e) in order to evaluate compliance with the <br /> Applicable Categorical Pretreatment Standards. For other SIUs, for which the <br /> City has adjusted its local limits to factor out dilution flows, the user shall measure <br /> the flows and concentrations necessary to evaluate compliance with the adjusted <br /> pretreatment standard(s). <br /> C. All sample results shall indicate the time, date and place of sampling, and methods <br /> of analysis, and shall certify that such sampling and analysis is representative of <br /> normal work cycles and expected pollutant discharges from the user. If a user <br /> sampled and analyzed more frequently than what was required in its wastewater <br /> discharge permit, using methodologies in 40 CFR Part 136, it must submit all <br /> results of sampling and analysis of the discharge as part of its self-monitoring <br /> report. <br /> 5.2 Analytical Requirements <br /> All pollutant analyses, including sampling techniques, shall be performed in accordance <br /> with the techniques prescribed in 40 CFR Part 136, unless otherwise specified in an <br /> applicable categorical pretreatment standard. If 40 CFR Part 136 does not contain <br /> sampling or analytical techniques for the pollutant in question, sampling and analyses must <br /> be performed in accordance with procedures approved by the EPA. <br /> All analyses performed to establish compliance and used in compliance reporting shall be <br /> performed by a laboratory accredited by the Washington State Department of Ecology, <br /> Quality Assurance Division in accordance with 173-50 WAC. Laboratories must be <br /> accredited for the analyses for which they are performing. <br /> 5.3 City Monitoring of User's Wastewater <br /> The City will follow the same procedures as outlined in Sections 5.1 and 5.2 of this <br /> ordinance. <br /> 34 <br />